Electrosynthesis of <i>gem</i>-Bisthioenamines from Vinylazides and Thiols
Electrosynthesis of gem -bisthioenamines from vinyl azides and thiols was performed. The reaction proceeds in undivided electrochemical cell equipped with platinum electrodes in DMSO-MeCN solution using NH<sub>4</sub>I as the supporting electrolyte and redox catalyst and current density of 20 mA/cm<sup>2</sup>. Yields of the target products are 32-58%.