DETERMINATION OF SULFUR MUSTARDS HYDROLYSIS PRODUCTS IN WATER USING GAS CHROMATOGRAPHY/MASS-SPECTROMETRY
A method for determination of sulfur mustards hydrolysis products in water was developed. Water samples were concentrated by a rotary evaporator to dryness. The residue was silylated by feri-butyldimethylsilyl-N-trifluoroacetamide. The detection limits ranged from 0,005 to 0,05 mkg/mL. The method can be used for quantitative analysis sulfur mustards hydrolysis products in water by gas chromatography/mass-spectrometry.